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Department Structure and Dynamics of Energy Materials
Program of the 6th X-ray School
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6th X-ray school, 28.11. - 02.12.2022, 10 a.m. - 4:30 p.m.
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MONDAY, 28.11.
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GENERAL INTRODUCTION I:
- Fundamentals of crystallography
- Fundamentals of X-ray diffraction
- Introduction into X-ray CoreLab
- Pattern indexation by hand
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TUESDAY, 29.11.
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GENERAL INTRODUCTION II:
- Elements of X-ray powder pattern, peak shapes, measuring strategies
- Crystallographic databases: ICSD + ICDD-PDF
- Applying Powder Cell to X-ray powder patterns
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WEDNESDAY, 30.11.
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HANDS-ON TRAINIG AND PATTERN ANALYSIS I:
- Instrument introduction
- Optics, detectors, sample carriers
- Sample preparation and measuring parameters
- Data conversion
- Phase analysis of XRD powder pattern using Bruker EVA software
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THURSDAY, 01.12.
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HANDS-ON TRAINIG AND PATTERN ANALYSIS II:
- Grazing incidence XRD
- Non-ambient X-ray diffraction
- Automatic indexation
- LeBail refinement using Fullprof suite
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FRIDAY, 02.12.
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HANDS-ON TRAINIG AND PATTERN ANALYSIS III:
- Grazing incidence XRD
- Non-ambient X-ray diffraction
- Sequential refinements
- Science talk
- Closing
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