SAXS LR020
Kleinwinkel-Röntgendiffraktion
Anwendungsbeispiele:- Nanopartikel, Polymere, Kolloide
- Energiematerialien: Heterogene Katalyse, Perovskite, poröse kohlenstoffhaltige Materialien
- in-situ / -operando Aanalyse von Materialien für Energieumwandlung und -speicherung
Instrument-Beschreibung
| Daten des Instruments | |
|---|---|
| Röntgenquelle und Optik | IμS HIGHBRILLIANCE Cu Microfocus X-ray source |
| Fluss | Photon flux >5*10^8 |
| Germaniumblende | Ge600 450μm |
| Detektor | DECTRIS PILATUS3 100K-M |
| Achsen | Jenaer Antriebstechnik THK Achsen; Sample holder with movement 160mm perpendicular to the beam direction in y and 200mm in x direction. |
| Steuerungssoftware | LabView with Python |
| Q Skala | 0.02 < Q < 0.7 Å^-1 |
| Probenhalter | Holder for solid samples and for 5 capillaries (liquid samples) |
| Beamstops | In three different sizes |
| Software zur Datenreduzierung | The "BerSAS" data reduction software package has been developed by Dr. Uwe Keiderling, and is constantly being expanded to offer new options and data treatment tools. It contains a set of programs for automated two-dimensional and one-dimensional reduction of large amounts of data files, and a set of graphical tools for data analysis, documentation, and publication. |
| Probenkammer | Vacuum up to 0.02 mbar |