BESSY II: Magnetic ‘microflowers’ enhance magnetic fields locally
The magnetic microstructure of the nickel-iron alloy leads to a compression of the field lines in the centre. © A. Palau/ICMAB
Two magnetic contrast maps. The cobalt rod is located in the centre of the microflower. © S. Valencia /HZB
A flower-shaped structure only a few micrometres in size made of a nickel-iron alloy can concentrate and locally enhance magnetic fields. The size of the effect can be controlled by varying the geometry and number of 'petals'. This magnetic metamaterial developed by Dr Anna Palau's group at the Institut de Ciencia de Materials de Barcelona (ICMAB) in collaboration with her partners of the CHIST-ERA MetaMagIC project, has now been studied at BESSY II in collaboration with Dr Sergio Valencia. Such a device can be used to increase the sensitivity of magnetic sensors, to reduce the energy required for creating local magnetic fields, but also, at the PEEM experimental station, to study samples under much higher magnetic fields than currently possible.
Dr Anna Palau from the Institut de Ciencia de Materials de Barcelona (ICMAB) has developed a special metamaterial that looks like tiny flowers under the scanning electron microscope. The 'petals' consist of strips of a ferromagnetic nickel-iron alloy. The microflowers can be produced in various geometries, not only with different inner and outer radii, but also with variable numbers and widths of petals. This flower-shaped geometry causes the field lines of an external magnetic field to concentrate in the centre of the device, resulting on a greatly intensified magnetic field.
Magnetic metamaterials
'Metamaterials are artificially produced materials with microstructures whose dimensions are smaller than the electromagnetic or thermal waves they are designed to manipulate,' explains Anna Palau. The physicist is working on magnetic microstructures that can be used in data storage, information processing, biomedicine, catalysis and magnetic sensor technology. By using these metamaterials, the sensitivity of magnetic sensors could be highly increased, as the magnetic field to be detected would be amplified at the center of these systems.
Mapping magnetic domains at BESSY II
Anna Palau, her student Aleix Barrera, and Sergio Valencia have now investigated this at the XPEEM experimental station at BESSY II. They placed a cobalt rod in the centre of various microflowers as a sensor for the magnetic field and mapped the magnetic domains inside the cobalt rod. 'By adjusting the geometric parameters such as shape, size and number of petals, the magnetic behaviour can be switched and controlled,' says Valencia. As a result, the sensitivity of a magnetoresistive sensor could be increased by more than two orders of magnitude.
New options, also for experiments at XPEEM
This innovation opens up new technological options for improving the performance of small magnetic sensors and for developing multifunctional magnetic components. In the future, such microstructures could be used to generate much higher magnetic fields locally, which is also of interest for the experimental XPEEM station at BESSY II. 'Our experimental system is a photoemission electron microscope, so magnetic fields deflect the electrons and make the experiments difficult,' says Valencia. 'The maximum magnetic field we can normally apply for imaging is about 25 millitesla (mT). With the magnetic field concentrator, where the field is only locally enhanced, we can easily achieve fields five times higher.' This is very exciting because it opens up the possibility of studying a range of magnetic systems under conditions that have not been possible before.
- BESSY II: Phosphorous chains – a 1D material with 1D electronic propertiesFor the first time, a team at BESSY II has succeeded in demonstrating the one-dimensional electronic properties of a material through a highly refined experimental process. The samples consisted of short chains of phosphorus atoms that self-organise at specific angles on a silver substrate. Through sophisticated analysis, the team was able to disentangle the contributions of these differently aligned chains. This revealed that the electronic properties of each chain are indeed one-dimensional. Calculations predict an exciting phase transition to be expected as soon as these chains are more closely packed. While material consisting of individual chains with longer distances is semiconducting, a very dense chain structure would be metallic.
- Did marine life in the palaeocene use a compass?Some ancient marine organisms produced mysterious magnetic particles of unusually large size, which can now be found as fossils in marine sediments. An international team has succeeded in mapping the magnetic domains on one of such ‘giant magnetofossils’ using a sophisticated method at the Diamond X-ray source. Their analysis shows that these particles could have allowed these organisms to sense tiny variations in both the direction and intensity of the Earth’s magnetic field, enabling them to geolocate themselves and navigate across the ocean. The method offers a powerful tool for magnetically testing whether putative biological iron oxide particles in Mars samples have a biogenic origin.
- What vibrating molecules might reveal about cell biologyInfrared vibrational spectroscopy at BESSY II can be used to create high-resolution maps of molecules inside live cells and cell organelles in native aqueous environment, according to a new study by a team from HZB and Humboldt University in Berlin. Nano-IR spectroscopy with s-SNOM at the IRIS beamline is now suitable for examining tiny biological samples in liquid medium in the nanometre range and generating infrared images of molecular vibrations with nanometre resolution. It is even possible to obtain 3D information. To test the method, the team grew fibroblasts on a highly transparent SiC membrane and examined them in vivo. This method will provide new insights into cell biology.