Only at BESSY II worldwide: IR nanoscopy at very long THz wavelengths
The schematic picture illustrates the range of wavenumbers which now is accessible with sSNOM at the IRIS-Beamline of BESSY II. © A.Veber/HZB
The team at the IRIS beamline at BESSY II has created a new experimental option: They achieved infrared nanoscopy with a spatial resolution of around 50 nm at very long THz wavelengths. This was possible thanks to a temporal pattern of light pulses known as the low-alpha operating mode at BESSY II. Worldwide, BESSY II is the only synchrotron light source at which users could perform nanoscopy in a single setup from 25 to 4000 cm-1, a unique opportunity for ultra-broadband characterisation of complex materials at the nanoscale in both the life sciences and materials sciences.
Near-field scanning microscopy (s-SNOM), based on infrared (IR) scattering, is a versatile analytical tool. The technique enables detailed chemical characterisation using IR spectroscopy far beyond the diffraction limit in the nanometre range. Modern tunable IR laser sources cover the spectral range from approximately 550 to 7000 cm⁻¹. Using synchrotron radiation sources, s-SNOM near-field spectroscopy is now possible down to 160 cm-1 or even 100 cm-1, whilst the range below < 100 cm-1 was previously not covered.
Now, a team led by Dr Alexander Veber has demonstrated at a commercially available s-SNOM system at the IRIS beamline at BESSY II experiments in the spectral range from 25 to 55 cm-1 and with a spatial resolution of 60 nm. The big advantage: The same optical configuration can now be used for nanoscopy in the range from 25 to 4000 cm-1. Conducting experiments across the THz, far-infrared and mid-infrared spectral ranges in a single setup offers a unique opportunity for ultra-broadband characterisation of complex materials at the nanoscale in both the life sciences and materials sciences.
The key condition is the so-called ‘low-alpha’ operating mode at BESSY II which offers a significant advantage in terms of flux and brilliance in the THz range. The extension of nanospectroscopy to the lower energy ranges enables the investigation of phenomena such as collective lattice vibrations, plasmonic oscillations, charge carriers and intermolecular interactions.
Note: The authors thank HZB-BESSY for the allocation of beam times at beamline IRIS. Funding by the German Federal Ministry for Education and Research (BMBF) project 05K19KH1 (SyMS) is gratefully acknowledged.
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